Effects of reaction conditions in microwave synthesis of nanocrystalline barium titanate

Sung Hwa Jhung; Jin Ho Lee; Ji Woong Yoon; Young Kyu Hwang; Jin Soo Hwang; Sang Eon Park; Jong San Chang

doi:10.1016/j.matlet.2004.06.006

Effects of reaction conditions in microwave synthesis of nanocrystalline barium titanate

Sung Hwa Jhung, Jin Ho Lee, Ji Woong Yoon, Young Kyu Hwang, Jin Soo Hwang, Sang Eon Park, Jong San Chang

Research output: Contribution to journal › Article › peer-review

50 Scopus citations

Abstract

The effect of synthesis parameters such as H₂O/Ti, Ba/Ti and OH^-/Ti ratios and heating methods (microwave irradiation and hydrothermal heating) on the synthesis of BaTiO₃ crystals has been investigated to prepare nanocrystalline BaTiO₃ crystals. The nanocrystals (less than 30 nm) were synthesized with microwave irradiation of reaction mixture prepared from conventional chloride precursors. The crystal size decreased with an increase of hydroxide and barium concentrations, whereas the size decreased with a decrease of the water concentration. Synthesis of BaTiO₃ with the microwave provided advantages of fast crystallization and decreased crystal size.

Original language	English
Pages (from-to)	3161-3165
Number of pages	5
Journal	Materials Letters
Volume	58
Issue number	25
DOIs	https://doi.org/10.1016/j.matlet.2004.06.006
State	Published - Oct 2004

Keywords

Barium titanate
Electroceramics
Microwave
Nanocrystal
Perovskites

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10.1016/j.matlet.2004.06.006

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title = "Effects of reaction conditions in microwave synthesis of nanocrystalline barium titanate",

abstract = "The effect of synthesis parameters such as H2O/Ti, Ba/Ti and OH-/Ti ratios and heating methods (microwave irradiation and hydrothermal heating) on the synthesis of BaTiO3 crystals has been investigated to prepare nanocrystalline BaTiO3 crystals. The nanocrystals (less than 30 nm) were synthesized with microwave irradiation of reaction mixture prepared from conventional chloride precursors. The crystal size decreased with an increase of hydroxide and barium concentrations, whereas the size decreased with a decrease of the water concentration. Synthesis of BaTiO3 with the microwave provided advantages of fast crystallization and decreased crystal size.",

keywords = "Barium titanate, Electroceramics, Microwave, Nanocrystal, Perovskites",

author = "Jhung, {Sung Hwa} and Lee, {Jin Ho} and Yoon, {Ji Woong} and Hwang, {Young Kyu} and Hwang, {Jin Soo} and Park, {Sang Eon} and Chang, {Jong San}",

year = "2004",

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doi = "10.1016/j.matlet.2004.06.006",

language = "English",

volume = "58",

pages = "3161--3165",

journal = "Materials Letters",

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T1 - Effects of reaction conditions in microwave synthesis of nanocrystalline barium titanate

AU - Jhung, Sung Hwa

AU - Lee, Jin Ho

AU - Yoon, Ji Woong

AU - Hwang, Young Kyu

AU - Hwang, Jin Soo

AU - Park, Sang Eon

AU - Chang, Jong San

PY - 2004/10

Y1 - 2004/10

N2 - The effect of synthesis parameters such as H2O/Ti, Ba/Ti and OH-/Ti ratios and heating methods (microwave irradiation and hydrothermal heating) on the synthesis of BaTiO3 crystals has been investigated to prepare nanocrystalline BaTiO3 crystals. The nanocrystals (less than 30 nm) were synthesized with microwave irradiation of reaction mixture prepared from conventional chloride precursors. The crystal size decreased with an increase of hydroxide and barium concentrations, whereas the size decreased with a decrease of the water concentration. Synthesis of BaTiO3 with the microwave provided advantages of fast crystallization and decreased crystal size.

AB - The effect of synthesis parameters such as H2O/Ti, Ba/Ti and OH-/Ti ratios and heating methods (microwave irradiation and hydrothermal heating) on the synthesis of BaTiO3 crystals has been investigated to prepare nanocrystalline BaTiO3 crystals. The nanocrystals (less than 30 nm) were synthesized with microwave irradiation of reaction mixture prepared from conventional chloride precursors. The crystal size decreased with an increase of hydroxide and barium concentrations, whereas the size decreased with a decrease of the water concentration. Synthesis of BaTiO3 with the microwave provided advantages of fast crystallization and decreased crystal size.

KW - Barium titanate

KW - Electroceramics

KW - Microwave

KW - Nanocrystal

KW - Perovskites

UR - http://www.scopus.com/inward/record.url?scp=4344606515&partnerID=8YFLogxK

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DO - 10.1016/j.matlet.2004.06.006

M3 - Article

AN - SCOPUS:4344606515

SN - 0167-577X

VL - 58

SP - 3161

EP - 3165

JO - Materials Letters

JF - Materials Letters

IS - 25

ER -

Effects of reaction conditions in microwave synthesis of nanocrystalline barium titanate

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