One-step synthesis of electrically conductive polyaniline nanostructures by oxidative polymerization method

Dhanusuraman Ragupathy; Palanisamy Gomathi; Soo Chool Lee; Salem S. Al-Deyab; Sang Hak Lee; Han Do Ghim

doi:10.1016/j.jiec.2012.01.032

One-step synthesis of electrically conductive polyaniline nanostructures by oxidative polymerization method

Dhanusuraman Ragupathy, Palanisamy Gomathi, Soo Chool Lee, Salem S. Al-Deyab, Sang Hak Lee, Han Do Ghim

Department of Textile System Engineering

Research output: Contribution to journal › Article › peer-review

35 Scopus citations

Abstract

A simple, rapid and efficient route to prepare polyaniline nanostructures (PANI-NS) by "one-step chemical oxidative polymerization" method is described. This method possesses advantages in terms of good yield, short reaction time, neat conditions and cost-effectiveness. The morphology of the PANI-NS was investigated by field-emission scanning electron microscopy (FE-SEM). The average diameter of single PANI-NS was calculated to be ∼376. nm. Results from UV-visible spectroscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis and cyclic voltammetry (CV) reveals the existence of PANI units present in the polymeric nanostructures. Also, electrical conducting property of the PANI-NS was analyzed using four-probe measurement method.

Original language	English
Pages (from-to)	1213-1215
Number of pages	3
Journal	Journal of Industrial and Engineering Chemistry
Volume	18
Issue number	4
DOIs	https://doi.org/10.1016/j.jiec.2012.01.032
State	Published - 25 Jul 2012

Keywords

Electrical
Nanostructures
Polyaniline
Polymerization
Surfactant

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10.1016/j.jiec.2012.01.032

Cite this

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title = "One-step synthesis of electrically conductive polyaniline nanostructures by oxidative polymerization method",

abstract = "A simple, rapid and efficient route to prepare polyaniline nanostructures (PANI-NS) by {"}one-step chemical oxidative polymerization{"} method is described. This method possesses advantages in terms of good yield, short reaction time, neat conditions and cost-effectiveness. The morphology of the PANI-NS was investigated by field-emission scanning electron microscopy (FE-SEM). The average diameter of single PANI-NS was calculated to be ∼376. nm. Results from UV-visible spectroscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis and cyclic voltammetry (CV) reveals the existence of PANI units present in the polymeric nanostructures. Also, electrical conducting property of the PANI-NS was analyzed using four-probe measurement method.",

keywords = "Electrical, Nanostructures, Polyaniline, Polymerization, Surfactant",

author = "Dhanusuraman Ragupathy and Palanisamy Gomathi and Lee, {Soo Chool} and Al-Deyab, {Salem S.} and Lee, {Sang Hak} and Ghim, {Han Do}",

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TY - JOUR

T1 - One-step synthesis of electrically conductive polyaniline nanostructures by oxidative polymerization method

AU - Ragupathy, Dhanusuraman

AU - Gomathi, Palanisamy

AU - Lee, Soo Chool

AU - Al-Deyab, Salem S.

AU - Lee, Sang Hak

AU - Ghim, Han Do

PY - 2012/7/25

Y1 - 2012/7/25

N2 - A simple, rapid and efficient route to prepare polyaniline nanostructures (PANI-NS) by "one-step chemical oxidative polymerization" method is described. This method possesses advantages in terms of good yield, short reaction time, neat conditions and cost-effectiveness. The morphology of the PANI-NS was investigated by field-emission scanning electron microscopy (FE-SEM). The average diameter of single PANI-NS was calculated to be ∼376. nm. Results from UV-visible spectroscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis and cyclic voltammetry (CV) reveals the existence of PANI units present in the polymeric nanostructures. Also, electrical conducting property of the PANI-NS was analyzed using four-probe measurement method.

AB - A simple, rapid and efficient route to prepare polyaniline nanostructures (PANI-NS) by "one-step chemical oxidative polymerization" method is described. This method possesses advantages in terms of good yield, short reaction time, neat conditions and cost-effectiveness. The morphology of the PANI-NS was investigated by field-emission scanning electron microscopy (FE-SEM). The average diameter of single PANI-NS was calculated to be ∼376. nm. Results from UV-visible spectroscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis and cyclic voltammetry (CV) reveals the existence of PANI units present in the polymeric nanostructures. Also, electrical conducting property of the PANI-NS was analyzed using four-probe measurement method.

KW - Electrical

KW - Nanostructures

KW - Polyaniline

KW - Polymerization

KW - Surfactant

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EP - 1215

JO - Journal of Industrial and Engineering Chemistry

JF - Journal of Industrial and Engineering Chemistry

IS - 4

ER -

One-step synthesis of electrically conductive polyaniline nanostructures by oxidative polymerization method

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Keywords

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