Palladium-catalyzed three-component cyclization of 2-bromocyclohex-1-enecarboxylic acids with carbon monoxide and arylhydrazines leading to 2-anilinohydroisoindoline-1,3-diones

Il Chul Yoon; Chan Sik Cho

doi:10.1002/aoc.3274

Palladium-catalyzed three-component cyclization of 2-bromocyclohex-1-enecarboxylic acids with carbon monoxide and arylhydrazines leading to 2-anilinohydroisoindoline-1,3-diones

Il Chul Yoon, Chan Sik Cho

Department of Applied Chemistry

Kyungpook National University

Research output: Contribution to journal › Article › peer-review

5 Scopus citations

Abstract

2-Bromocyclohex-1-enecarboxylic acids are carbonylatively cyclized with arylhydrazines or their hydrochlorides in tetrahydrofuran at 120 °C under carbon monoxide pressure in the presence of a catalytic amount of PdCl₂ and 1,3-bis(diphenylphosphino)propane along with Et₃N to give 2-anilinohydroisoindoline-1,3-diones.

Original language	English
Pages (from-to)	226-230
Number of pages	5
Journal	Applied Organometallic Chemistry
Volume	29
Issue number	4
DOIs	https://doi.org/10.1002/aoc.3274
State	Published - Apr 2015

Keywords

2-anilinohydroisoindoline-1 3-diones
2-bromocyclohex-1-enecarboxylic acids
arylhydrazines
carbonylation and cyclization
palladium catalyst

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title = "Palladium-catalyzed three-component cyclization of 2-bromocyclohex-1-enecarboxylic acids with carbon monoxide and arylhydrazines leading to 2-anilinohydroisoindoline-1,3-diones",

abstract = "2-Bromocyclohex-1-enecarboxylic acids are carbonylatively cyclized with arylhydrazines or their hydrochlorides in tetrahydrofuran at 120 °C under carbon monoxide pressure in the presence of a catalytic amount of PdCl2 and 1,3-bis(diphenylphosphino)propane along with Et3N to give 2-anilinohydroisoindoline-1,3-diones.",

keywords = "2-anilinohydroisoindoline-1 3-diones, 2-bromocyclohex-1-enecarboxylic acids, arylhydrazines, carbonylation and cyclization, palladium catalyst",

author = "Yoon, {Il Chul} and Cho, {Chan Sik}",

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year = "2015",

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doi = "10.1002/aoc.3274",

language = "English",

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AU - Yoon, Il Chul

AU - Cho, Chan Sik

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N2 - 2-Bromocyclohex-1-enecarboxylic acids are carbonylatively cyclized with arylhydrazines or their hydrochlorides in tetrahydrofuran at 120 °C under carbon monoxide pressure in the presence of a catalytic amount of PdCl2 and 1,3-bis(diphenylphosphino)propane along with Et3N to give 2-anilinohydroisoindoline-1,3-diones.

AB - 2-Bromocyclohex-1-enecarboxylic acids are carbonylatively cyclized with arylhydrazines or their hydrochlorides in tetrahydrofuran at 120 °C under carbon monoxide pressure in the presence of a catalytic amount of PdCl2 and 1,3-bis(diphenylphosphino)propane along with Et3N to give 2-anilinohydroisoindoline-1,3-diones.

KW - 2-anilinohydroisoindoline-1 3-diones

KW - 2-bromocyclohex-1-enecarboxylic acids

KW - arylhydrazines

KW - carbonylation and cyclization

KW - palladium catalyst

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DO - 10.1002/aoc.3274

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VL - 29

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JO - Applied Organometallic Chemistry

JF - Applied Organometallic Chemistry

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ER -

Palladium-catalyzed three-component cyclization of 2-bromocyclohex-1-enecarboxylic acids with carbon monoxide and arylhydrazines leading to 2-anilinohydroisoindoline-1,3-diones

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